Nuclear Magnetic Resonance Volume 25

A Review of the Literature Published Between June 1994 and May 1995

By G. A. Webb

The Royal Society of Chemistry

Copyright © 1996 The Royal Society of Chemistry
All rights reserved.
ISBN: 978-0-85404-307-1

Contents

CHAPTER 1 NMR Books and Reviews By G. G. Webb, 1,
CHAPTER 2 Theoretical and Physical Aspects of Nuclear Shielding By C. J. Jameson, 38,
CHAPTER 3 Applications of Nuclear Shielding By M. Yamaguchi, 83,
CHAPTER 4 Theoretical Aspects of Spin-Spin Couplings By H. Fukui, 152,
CHAPTER 5 Applications of Spin-Spin Couplings By K. Kamienska-Trela and J. Wojcik, 177,
CHAPTER 6 Solid-State NMR By J. R. Agger and M. W. Anderson, 229,
CHAPTER 7 Multiple Pulse NMR By L. Y. Lian, 272,
CHAPTER 8 Natural Macromolecules By J. R. P. Arnold and J. Fisher, 298,
CHAPTER 9 Synthetic Macromolecules By A. H. Fawcett, 350,
CHAPTER 10 Conformational Analysis By T. J. Rutherford, 361,
CHAPTER 11 Nuclear Magnetic Resonance Spectroscopy of Living Systems By M. J. W. Prior, 404,
CHAPTER 12 Nuclear Magnetic Resonance Imaging By A.R.C. Gates, 429,
CHAPTER 13 Oriented Molecules By C. L. Khetrapal and K. V. Ramanathan, 455,
Author Index, 480,

CHAPTER 1

NMR Books and Reviews

Compiled by G. A. WEBB

The section lists all books and reviews, with NMR as the principal theme, that were known to the compiler for the period under review. In most cases the source of references is the ‘CA Selects–NMR Chemical Aspects’ listings from the period from June 1994 to May 1995. References to technical bulletins, company or institute house journals, special reports, etc., are normally omitted. In general, texts of individual lectures from symposia are not listed nor are NMR sections of general chemistry or spectroscopy textbooks. The compilation is sectionalized for the reader’s convenience. The foreign language articles are grouped together according to language and the English title is provided.

1 Books

R1 R. Y. Dong, ‘NMR of Liquid Crystals’, Springer, Berlin, 1994, 260 pp

2 Regular Review Series

Advances in Chemical Physics, 1993, vol. 85

R2 M. W. Evans, ‘Laser and Pulsed-Laser NMR Spectroscopy’, p. 51

Advances in Chemistry Series, 1994, vol. 234

R3 K. K. Unger, ‘Surface Structure of Amorphous and Crystalline Porous Silicas’, p. 165

R4 G. E. Maciel, C. E. Bronnimann, R. C. Zeigler, I. S. Chuang, D. R. Kinneis and E. A. Keiter, ‘Multinuclear NMR Spectroscopic Studies of Silica Surfaces’, p. 269

Advances in Spectroscopy, 1993, vol. 22

R5 P. J. Barrie, ‘Solid State NMR Studies of Aluminophosphate Based Molecular Sieves’, p. 151

R6 T. Mitani and T. Inabe, ‘Spectroscopy of Proton and Electron Cooperative Systems’, p. 291

Advances in Magnetic and Optical Resonance, ed. W. S. Warren, 1994, vol. 18

R7 B. H. Meier, ‘Polarization Transfer and Spin Diffusion in Solid State NMR’, p. 1

R8 F. C. Spano and J. Knoester, ‘Fermions on a Frenkel Chain’, p. 117

Annual Reports on NMR Spectroscopy, ed. G. A. Webb, 1994, vol. 29

R9 A. C. de Dios and C. J. Jameson, The NMR Chemical Shift: Insight into Structure and Environment’, p. 1

R10 D. B. Chesnut, ‘Ab Initio Calculations of NMR Chemical Shielding’, p. 71

R11 T. A. Cross, ‘Structural Biology of Peptides and Proteins in Synthetic Membrane Environments by Solid-State NMR Spectroscopy’, p. 123

R12 I. S. Chuang and G. E. Maciel, ‘NMR Characterisation of Complex Organic Resins’, p. 169

R13 G. Moad, ‘Applications of Labelling and Multidimensional NMR Characterisation of Synthetic Polymers’, p. 287

R14 T. Asakura, M. Demura and T. Hayashi, ’13C NMR Assignments of Polyolefines and Olefine Copolymers Based on the 13C NMR Chemical Shift Calculations and 2D INADEQUATE NMR’, p. 325

1995, vol. 30

R15 J. D. Augspurger and C. E. Dykstra, ‘Calculation and Prediction of Structural NMR Shifts in Respiratory Proteins’, p. 1

R16 P. J. Barrie, ‘NMR Applications to Porous Solids’, p. 37

R17 K. Takegoshi, ‘Miscibility, Morphology and Molecular Motion in Polymer Blends’, p. 97

R18 K. Kamienska-Trela, ‘One Bond 13C–13C Spin-Spin Coupling Constants’, p. 131

R19 M. Budesinsky and D. Saman, ’13C NMR Spectra of Sesquiterpene Lactones’, p. 232

Annual Reports on Progress in Chemistry, 1993, vol. 89, Section B

R20 A. M. Chippendale, ‘NMR Spectroscopy’, p. 3

vol. 89, Section C

R21 G. A. Webb, ‘NMR Specroscopy’, p. 3

1994, vol. 90, Section B

R22 A. M. Chippendale, ‘NMR Spectroscopy’, p. 3

Annual Reviews of Biophysics and Biomolecular Structure, 1994, vol. 23

R23 J. Jonas and A. Jonas, ‘High Pressure NMR Spectroscopy of Proteins and Membranes’, p. 287

Annual Reviews of Physical Chemistry, 1994, vol. 45

R24 S. J. Opella, ‘Solid State NMR Structural Studies of Proteins’, p. 659

Bulletin of Magnetic Resonance, 1994, vol. 16

R25 R. R. Ernst, ‘NMR Fourier Transform Spectroscopy’, p. 5

R26 A. Kumar, ‘Reminiscences of My Journey Through a ‘Nobel’ Lab.’, p. 33

R27 J. Jeener, ‘Emphasizing the Role of Time in Quantum Dynamics’, p. 35

R28 J. Weber, F. Herrmann, P. Roesch and A. Wokaun, ‘A Novel Contour Plot Algorithm for the processing of 2D and 3D NMR Spectra’, p. 43

R29 O. W. Sorensen, ‘Selective Rotations Using Non-Selective Pulses and Heteronuclear Couplings’, p. 49

R30 M. Ranee, ‘Sensitivity Improvement in Multi-Dimensional NMR Spectroscopy’, p. 54

R31 S. L. Gann, J. H. Baltisberger, E. W. Wooten, H. Zimmermann and A. Pines, ‘Cross Polarization and Dynamic Angle Spinning of 0 in L-Alanine’, p. 68

R32 S. Macura, J. Fejzo, W. M. Westler and J. L. Markley, ‘Influence of Slow Internal Motion in Proteins on Cross Polarization Rates Determined by Two Dimensional Exchange Spectroscopy’, p. 73

R33 M. H. Levitt and L. Di Bari, ‘The Homogeneous Master Equation and the Manipulation of Relaxation Networks’, p. 94

R34 P. K. Madhu, R. Christy, R. Grace and A. Kumar, ‘Effects of Cross Correlations in 2D NOE Experiments’, p. 115

R35 D. C. Newitt and E. L. Hahn, ‘Detection of Two Quantum Nuclear Coherence by Nuclear Quadrupole Induced Electric Polarization’, p. 127

Chemical Reviews, 1994, vol. 94

R36 D. H. Busch and N. W. Alcock, ‘Iron and Cobalt Lacunar Complexes as Dioxygen Carriers’, p. 585

R37 M. Momenteau and C. A. Reed, ‘Synthetic Heme Dioxygen Complexes’, p. 659

R38 D. G. Gorenstein, ‘Conformation and Dynamics of DNA and Protein DNA Complexes by 31P NMR’, p. 1315

R39 P. W. Jennings and L. L. Johnson, ‘Metallocyclobutane Complexes of the Group 8 Transition Metals’, p. 2241

1995, vol. 95

R40 V. Alexander, ‘Design and Synthesis of Macrocyclic Ligands and Their Complexes of Lanthanides and Actinides’, p. 273

Chemical Society Reviews, 1994, vol. 23

R41 T. J. Norwood, ‘Magnetic Field Gradients in NMR: Friend or Foe?’, p. 59

R42 D. W. Young, ‘Studies on Thymidylate Synthase and DHR’, p. 119

R43 A. Sacco, ‘Structure and Dynamics of Electrolyte Solutions’, p. 129

R44 M. Holz, ‘Electrophoretic NMR’, p. 165

Coordination Chemistry Reviews, 1994, vol. 130

R45 A. Haas, ‘Te and Se Nitrogen Compounds’, p. 301

R46 S. Walter, ‘From Aminosilane to Iminosilane’, p. 481

1994, vol. 133

R47 J. Barker and M. Kilner, ‘The Coordination Chemistry of the Amidine Ligand’, p. 219

1994, vol. 135

R48 Y. Dong, ‘Coordination Chemistry of Cyclopentadienyl Titanium Carboxylates and Related Complexes’, p. 93

NMR Basic Principles and Progress, ed. P. Diehl, S. Fluck, H. Guenther,

R. Kosfeld and J. Seelig, 1994, vol. 31

R49 G. Engelhardt and H. Koller, ’29Si NMR of Inorganic Solids’, p. 1

R50 H. Pfeifer, ‘NMR of Solid Surfaces’, p. 31

R51 A. Sebald, ‘MAS and CP/MAS NMR of Less Common spin 1/2 Nuclei’, p. 91

R52 C. Jaeger, ‘Satellite Transition Spectroscopy of Quadrupolar Nuclei’, p. 133

R53 D. Brinkmann and M. Mali, ‘NMR and NQR Studies of High Temperature Superconductors’, p. 171

1994, vol. 32

R54 G. L. Hoatson and R. L. Void, ‘2H NMR Spectroscopy of Solids and Liquid Crystals’, p. 1

R55 D. Michel and F. Engelke, ‘Cross Polarization, Relaxation Times and Spin Diffusion in Rotating Solids’, p. 69

R56 W. S. Veeman and W. E. J. R. Maas, ‘Solid State NMR Techniques for the Study of Polymer-Polymer Miscibility’, p. 127

R57 H. W. Beckham and H. W. Spiess, ‘2D Exchange NMR Spectroscopy in Polymer Research’, p. 163

Progress in NMR Spectroscopy, ed. J. W. Emsley, J. Feeney and L. H. Sutcliffe, 1994, vol. 26

R58 I. P. Gerothanassis, ‘Multinuclear and Multidimensional NMR Methodology for Studying Individual Water Molecules Bound to Peptides and Proteins in Solution’, p. 171

R59 I. P. Gerothanassis, ‘0 NMR Studies of Hemoproteins and Synthetic Model Compounds in Solution and Solid States’, p. 239

R60 J. T. Gerig, ‘Fluorine NMR of Proteins’, p. 293

R61 D. M. LeMaster, ‘Isotope Labeling in Solution Protein Assignments and Structural Analysis’, p. 371

R62 C. R. Sanders, B. J. Hure, K. P. Howard and J. H. Prestegard, ‘Magnetically Oriented Phospholipid Micelles as a Tool for the Study of Membrane Associated Molecules’, p. 421

R63 O. Soderman and P. Stilbs, ‘NMR Studies of Complex Surfactant Systems’, p. 445

R64 G. Lindblom and G. Oraedd, ‘NMR Studies of Translational Diffusion in Lyotropic Liquid Crystals and Lipis Membranes’, p. 483

R65 F. Ni, ‘Recent Developments in Transferred NOE Methods’, p. 517

1995, vol. 27

R66 H. Duddeck, ’77Se NMR Spectroscopy’, p. 1

Spectroscopic Properties of Inorganic and Organometallic Compounds, ed.

G. Davidson, 1994, vol. 27

R67 B. E. Mann, ‘NMR Spectroscopy’, p. 1

3 Edited Books and Symposia

ACS Symposia Series

R68 T. Asakura, M. Demura, A. Uyama, K. Ogawa, K. Komatsu, L. K. Nicholson and T. A. Cross, ‘NMR Characterisation of Silk Proteins’, 1994, 544, 148

R69 C. J. Hapeman.’Oxidation of s-Triazine Pesticides’, 1994, 554, 223

R70 R. P. Hughes, O. J. Curnow, P. R. Rose, X. Zheng, E. N. Mairs and A. L. Rheingold, ‘New and Revisited Transition Metal Chemistry of Fluoroolefins and Fluorodienes’, 1994, 555, 252

R71 P. J. Toscano, E. Barren, H. Brand, L. Konieczny, J. E. Schermerhan, K. Shufan and S. van Winhler, ‘NMR Studies’, 1994, 555, 286

R72 G. R. Choppin and P. J. Wang, ‘Lanthanide Aminopolycarboxylates’, 1994, 565, 346

R73 R. J. Woods, B. Fraser-Reid, R. A. Dwek and C. J. Edge, ‘Role of Nonbonded Interactions in Determining Solution Conformations of Oligosaccharides’, 1994, 569, 252

R74 M. Hanack, ‘Transition Metallophthalocyanines as Structures for Materials Design’, 1994, 572, 472

R75 I. C. Baianu, E. M. Ozu, T. C. Wei and T. F. Kumosinski, ‘Molecular Dynamics and NMR Studies of Concentrated Electrolytes and Dipoles in Water’, 1994, 576, 269

R76 R. H. Griffey, E. Lesnik, S. Freier, Y. S. Sanghvi, K. Teng, A. Kawasaki, C. Guinasso, P. Wheeler and V. Mohan, ‘New Twists on Nucleic Acids’, 1994, 580, 212

Advances in Botanical Research

R77 R. G. Ratcliffe, ‘In vivo NMR Studies of Higher Plants and Algae’, 1994, 20, 43

Advances in Lipid Methodology, ed. W. W. Christie, Oily Press, Dundee, 1993, vol. 2

R78 F. D. Gunstone, ‘High Resolution 13C NMR Spectroscopy of Lipids’, p. 1

R79 B. A. Kelly, M. E. Rose and D. S. Millington, ‘Analysis of Acyl Carnitines’, p. 247

Advances in Neutron Capture Therapy, ed. A. H. Soloway, R. F. Barth and D. E. Carpenter, Plenum Press, New York, 1993

R80 A. Corder, A. Whittaker, D. Kelly, H. Meriaty, B. Allen and R. Martin, ‘Evaluation of a B Labelled DNA Ligand’, p. 377

R81 P. Tang, M. Schweizer, W. Bauer and K. Bradshaw, ‘NMR Studies of the Interaction of Borocaptate Sodium with Serum Albumin’, p. 453

R82 G. Kabalka, G. Cheng, C. Anderson, P. Bendel, P. Micca and D. Slatkin, ‘In vivo Pharmacokinetics of a Boron Neutron Capture Agent in a Tumor-bearing Rat via B MRS and MRT, p. 491

R83 K. Bradshaw, M. Schweizer, G. Glover and J. Hadley, ‘Pharmacokinetics of Borocaptate Sodium in Canine Head Determined by 11B MRI and Spectroscopy’, p. 579

Advances in NMR Studies of Polymeric Materials, ed. H. N. Cheng and T. A. Early, Huethig and Wepf, Zug, 1994

R84 H. N. Cheng and T. A. Early, ‘NMR Studies of Polymeric Materials-An Overview’, p. 1

R85 P. L. Rinalsi, L. Li, D. R. Hensley, D. G. Ray and H. J. Harwood, ‘Applications of Triple Resonance NMR Techniques to the Study of Polymer Structure and Reactivity’, p. 15

R86 K. Beshah, ‘Sequence Identification of Polymer Microstructures by Hetero- nuclear NMR Correlations’, p. 35

R87 E. F. McCord, W. L. Anton, L. Wilczek, S. D. Ittel, L. T. J. Nelson, K. D. Raffell, J. E. Hansen and C. Berge, ‘1H and 13C NMR of PMMA Macromonomers and Oligomers–End Groups and Tacticity’, p.47

R88 G. M. Benedikt, B. L. Goodall, L. F. Rhodes and A. C. Kemball, ‘NMR Spectroscopy of Poly(vinyl chloride) Defects’, p. 65

R89 H. N. Cheng, ’13C NMR Sequence Determination and Modelling of Polypropylene Oils’, p. 77

R90 R. A. Newmark and G. N. Babu, ‘Sequence Analysis and Kinetic Study of the Polymerization of l,4-Bis(hydroxydimethylsilyl)Benzene with SiR2Cl2’, p. 103

R91 T. G. Neiss and E. W. Vanderheiden, ‘Solution and Solid State NMR Analysis of Phenolic Resin Cure Kinetics’, p. 117

R92 F. C. Schilling, T. W. Weidman and A. M. Joshi, ‘Solid State Characterisation of Polysilanes Containing the Si–H Bond’, p. 131

R93 M. J. Sullivan, ‘The Analysis of Heterogeneous Polymer Systems using Solid State NMR’, p. 145

R94 F. D. Blum, ‘Dynamics of the Interface in a Model Composite System’, p. 161

R95 D. G. Rethwisch, J. Van Alsten and C. R. Dybowski, ‘NMR Measurement of the Surface Dynamics of Poly(dimethylsiloxane) Adsorbed on Silica Gel’, p. 171

R96 P. A. Mirau, J. L. White and S. A. Heffner, ‘Intermolecular Interactions in Polymer Blends: ID and 2D NMR Studies’, p. 181

R97 P. B. Smith, D. T. DeLassus, A. S. Ellaboudy, D. E. Diedering, B. G. Landes, S. L. Anderson and E. A. Grulke, ‘Solid State NMR Investigation of Antiplasticization of Polystyrene by Mineral Oil’, p. 193

R98 R. C. Zeigler, ‘Dynamics of Polypropene and Propene-Ethylene Copolymers at Temperatures above Ambient’, p. 213

R99 P. P. J. Chu and J. J. Howard, ‘Nuclear Spin Relaxation Times Dispersion in Disordered Polymer Systems’, p. 229

R100 J. J. Marcinko and A. A. Parker, ‘An Overview of the Correlations between NMR Cross-Polarization Time Constants and Dynamic Moduli’, p. 251

R101 D. G. Cory, J. B. Miller and A. N. Garroway, ‘Chemically Resolved Solid State NMR Images of Polymers’, p. 259

R102 M. A. Hepp and J. B. Miller, ‘NMR Imaging of Solid Polymers: Strategies for Chemical Shift Selectivity’, p. 271

R103 J. L. Koenig, ‘NMR Imaging of Elastomeric Polymers’, p. 283

R104 S. W. Sinton, A. W. Chow and J. H. Iwamiya, ‘NMR Imaging as a New Tool for Rheology’, p. 299

American Institute of Physics Conference Proceedings, 1994, vol. 293

R105 A. Honig, N. Alexander, Q. Fan, X. Wei and Y. Y. Yu, ‘Achievement of Transportable Polarized D in Solid HD’, p. 50

1994, vol. 298

R106 H. H. Limbach, G. Scherer, L. Meschede, F. Aguilar-Parrilla, B. Wehrle, J. Braun, C. Hoelger and H. Benedict, ‘NMR Studies of Elementary Steps of Hydrogen Transfer in Condensed Phases’, p. 225

Alfred Benzon Symposia 1994, vol. 36

R107 R. J. Woods, C. J. Edge, M. R. Wormald and R. A. Dwek, ‘Glycom 93’, p. 15

R108 J. F. G. Vliegenthart, ‘Studies on the Carbohydrate Chains of Glycoproteins’, p. 30

Bioactive Natural Products, ed. S. M. Colegate and R. J. Molyneux, CRC, Boca Raton, 1993

R109 L. T. Byrne, ‘NMR Spectroscopic Strategies for Structural Determination’, p. 75

Cellulosics: Chemical, Biochemical and Material Aspects, ed. J. F. Kennedy,

G. O. Phillips and P. A. Williams, Ellis Horwood, London, 1993

R110 J. C. Roberts and J. Tatham, ‘The Application of 13C Solid State NMR to the Study of Surface Reactions of Cellulose with Succinic Anhydride’, p. 141

R111 J. T. Guthrie and R. D. Hirst, ‘The Characterisation of Cellulose Copolymer Carbanilates by 13C NMR Spectroscopy-Solution and Solid State Studies’, p. 153

R112 R. Tanaka, J. Meadows, P. A. Williams and G. O. Phillips, ‘A Spin Probe Study of the Interaction of Hydrophobically Modified Hydroxyethyl Cellulose with Sodium Dodecyl Sulfate’, p. 297

R113 J. R. Wright and L. J. Mathias, ‘New Lightweight Composites’, p.459

R114 D. J. Gardner, D. W. Gunnells, M. P. Wolcott and L. Amos, ‘Changes in Wood Polymers During the Pressing of Wood Composites’, p. 513

R115 H. Hatakeyama, S. Hirose, K. Nakamura and T. Hatakeyama, ‘New Types of Polyurethanes Derived from Lignocellulose and Saccharides’, p. 525

(Continues…)Excerpted from Nuclear Magnetic Resonance Volume 25 by G. A. Webb. Copyright © 1996 The Royal Society of Chemistry. Excerpted by permission of The Royal Society of Chemistry.
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