Nuclear Magnetic Resonance Volume 24

A Review of the Literature Published Between June 1993 and May 1994

By G. A. Webb

The Royal Society of Chemistry

Copyright © 1995 The Royal Society of Chemistry
All rights reserved.
ISBN: 978-0-85404-302-6

Contents

CHAPTER 1 NMR Books and Reviews Compiled by G.A. Webb, 1,
CHAPTER 2 Theoretical and Physical Aspects of Nuclear Shielding By C.J. Jameson, 44,
CHAPTER 3 Applications of Nuclear Shielding By M. Yamaguchi, 76,
CHAPTER 4 Theoretical Aspects of Spin-Spin Couplings By H. Fukui, 133,
CHAPTER 5 Applications of Spin-Spin Coupling Constants By K. Kamienska-Trela and J. Wójcik, 162,
CHAPTER 6 Nuclear Spin Relaxation in Liquids and Gases By H. Weingärtner, 209,
CHAPTER 7 Solid State NMR By M. W. Anderson, 233,
CHAPTER 8 Multiple Pulse NMR By L. Y. Lian, 273,
CHAPTER 9 Natural Macromolecules By J.R.P. Arnold and J. Fisher, 298,
CHAPTER 10 Synthetic Macromolecules By A.H. Fawcett, 334,
CHAPTER 11 Conformational Analysis By J. Barber and B. Wood, 362,
CHAPTER 12 Nuclear Magnetic Resonance Spectroscopy of Living Systems By M.J.W. Prior, 398,
CHAPTER 13 Nuclear Magnetic Resonance Imaging By S.C.R. Williams, 444,
CHAPTER 14 NMR of Paramagnetic Species By R.R. Sharp, 469,
CHAPTER 15 NMR of Liquid Crystals and Micellar Solutions By A. Khan, 514,
Author Index, 547,

CHAPTER 1

NMR Books and Reviews

COMPILED BY G. A. WEBB

This section lists all books and reviews, with NMR as the principal theme, that were known to the compiler, for the period under review. In most cases the source of reference is the ‘CA Selects-NMR Chemical Aspects’ listings for the period from June 1993 to May 1994. References to technical bulletins, company or institute house journals, special reports, etc., are normally omitted. In general, texts of individual lectures from symposia are not listed nor are NMR sections of general chemistry or spectroscopy textbooks. The compilation is sectionalized for the reader’s convenience. The foreign language articles are grouped together according to language and the English title is provided.

(a) BOOKS

R1 J.W. Hennel and J. Klinowski, “Fundamentals on NMR”, Longman, London, 1993, 288pp

R2 C. Jones, B. Mulloy and A.H. Thomas, “Spectroscopic Methods and Analyses”, Humana, Totowa, 1993, 395pp

(b) REGULAR REVIEW SERIES

Accounts of Chemical Research, 1993, vol.26

R3 H.G. Floss and S. Lee, “Chiral Methyl Groups: Small is Beautiful”, p.116

R4 A. Bax and S. Grzesiek, “Methodological Advances in Protein NMR”, p. 131

R5 D.B. Collum, “Solution Structures of Lithium Dialkylamides and related N-Lithiated Species”, p.227

Advances in Chemistry Series, 1993, vol.229

R6 R.A. Wind, G.E. Maciel and R.E. Botto, “Quantitation in 13C NMR Spectroscopy of Carbonaceous Solids”, p.3

R7 G.E. Maciel, C.E. Bronnimann and C.F. Ridenour, “1H NMR Spectroscopy: Approaches for Carbonaceous Solids”, p.27

R8 R.A. Wind, R. Lewis. H. Lock and G.E. Maciel,” Solid Materials research with NMR and Dynamic Nuclear Polarization Spectroscopy”, p.45

R9 H. Thomann and M. Bemardo, “Advances in Electron Nuclear Double Resonance Spectroscopy”, p.65

R10 M.K. Bowman, “Strategies for Measurement of Electron Spin Relaxation”, p.91

R11 R.L. Belford and R.B. Clarkson, “Multifrequency Electron Paramagnetic Resonance Spectroscopy”, p.107

R12 Y. Sanada and L.J. Lynch, “High Temperature ESR and NMR Methods Applied to Coal”, p.139

R13 W.A. Barton, L.J. Lynch, D.S. Webster and G. Simms, “Diffusion Coupled Relaxation and the Submicroscopic Structure of Bituminous Coals”, p.175

R14 A.M. Vassallo, “13C NMR Spectroscopy of Pyridine and Alkylpyridines Sorbed onto Coal”, p.201

R15 R.A. Wind, “Distortion Free 13C NMR Spectroscopy in Coal”, p.217

R16 R. Sakurovs, L.J. Lynch and W.A. Barton, “1H NMR Thermal Analysis of Argonne Premium Coals”, p.229

R17 D.E. Axelson, “Multivariate Statistical Analysis and Pattern Recognition”, p.253

R18 Y. Adachi and M. Nakamizo, “Structural Parameters of Argonne Coal Samples: Solid State 13C NMR Spectroscopy”, p.269

R19 N. Cyr and N.O. Egiebor,” Characterization of Coal Liquefaction Residues by Solid State 13C NMR Spectroscopy”, p.281

R20 K. Hayamizu, S. Hayashi, K. Kamiya and M. Kawamura, “1H NMR Spectroscopy and Spin-Lattice Relaxation of Argonne Premium Coals”, p.295

R21 J. Hu, L. Li and C. Ye, “High Field NMR Studies of Argonne Premium Coals”, p.323

R22 J.A. MacPhee, H. Kawashima, Y. Yamashita and Y. Yamada, “Solid State 13C NMR Studies on Coal and Coal Oxidation”, p.323

R23 C. Tsiao and R.E. Botto,” Measurement of Spin-Lattice Relaxation in Argonne Premium Coal Samples”, p.341

R24 L.D. Rosa, M. Pruski and B. Gerstein, “Quantitation of Protons in the Argonne Premium Coals by Solid State 1H NMR Spectroscopy”, p359

R25 J.A. Franz and J.C. Linehan, “Bloch Decay and Cross Polarization-Magic Angle Spinning 13C NMR Study of the Argonne Premium Coals; Effects of High Speed Spinning”, p.377

R26 A. Jurkiewicz, C.E. Bronnimann and G.E. Maciel,” High Resolution 1H NMR Studies of Argonne Premium Coals”, p.401

R27 A.M. Orendt, M.S. Solum, N.K. Sethi, C.D. Hughes, R.J. Pugmire and D.M. Grant, “Measurement of ^C Chemical Shielding Anisotropy in Coal”, p.419

R28 B.G. Silbemagel and R.E. Botto,” Advanced Magnetic Resonance Techniques Applied to Argonne premium Coals”, p.629

Advances in Experimental and Medical Biology, 1992, vol.316

R29 R. Vink, “NMR Spectroscopy and the Study of Tissue Oxygen Metabolism”, p.316

Annual Reports on Medicinal Chemistry, 1992, vol.27

R30 J.W. Erickson and S.W. Fesik, “Macromolecular X Ray Crystallography and NMR as Tools for Structure Based Drug Design”, p.271

Annual Reports on NMR Spectroscopy, ed. G.A. Webb, 1993, vol.27

R31 J. Cavanagh and M. Rance,” Sensitivity Enhanced NMR Techniques for the Study of Biomolecules”, p.1

R32 Y. Inoue, “NMR Studies of the Structure and Properties of Cyclodextrins and Their Inclusion Complexes”, p.59

R33 K.G. Orrell and V.Sik, “Dynamic NMR Spectrosocopy in Inorganic and Organometallic Chemistry”, p.103

R34 C.E. Mountford, C.L. Lean, W.B. Mackinnon and P. Russell, “The use of Proton MR in Cancer Pathology”, p.173

R35 T. Nose, “Pulsed Reid Gradient NMR Studies of the Diffusion of Chain Molecules in Polymer Matrices”, p.217

R36 R.H. Contreras and J.C. Facelli, “Advances in Theoretical and Physical Aspects of Spin-Spin Coupling Constants”, p.255

1994, vol.28

R37 H. Kawazoe, “Application of NMR Spectroscopy to the Science and Technology of Glasses and Ceramics”, p.1

R38 S. Hayashi,” High Resolution Solid State NMR Studies on Ceramics”, p.29

R39 H. Pfeifer and H. Ernst,” NMR Studies of Zeolites”, p.91

R40 H. Kurosu, S. Ando, H. Yoshimizu and I. Ando,” NMR Studies of Higher Order Structures of Solid Polymers”, p.189

R41 F.D. Blum, “NMR Studies of Organic Thin Films”, p.277

Annual Reports on Progress in Chemistry, Sect.B, 1991, vol.87

R42 J.R. Everett and S.A. Redshaw, “NMR Studies on the Structures of Carbohydrates”, p.3

1992, vol.88

R43 J.R. Everett and S.A. Redshaw, “NMR Studies on the Structure and Dynamics of Nucleic Acids and Their Complexes with Ions and Other Molecules”, p.3 Sect. C, 1993, vol. 89

R44 G.A. Webb, “NMR Spectroscopy”, p.3

Annual Reviews of Biochemistry, 1993, vol.62

R45 J.A. Jaeger, J. Santa Lucia and i.Tinoco,” Determination of RNA Structure and Thermodynamics”, p.255

Annual Reviews of Biophysics and Biomolecular Structure 1993, vol.22

R46 W, Chiu, “What does Electron Cryomicroscopy Provide that X Ray Crystallography and NMR Spectroscopy Cannot?”, p.233

Biological Magnetic Resonance, ed. L.J. Berliner and J. Reuben, 1992, vol.11

R47 L. Bolinger and R.E. Lenkinski, “Localization in Clinical NMR Spectroscopy”, P-1

R48 T. Schleich, G.H. Craines and J.M. Rydzewski, “Off Resonance Rotating Frame Spin-Lattice Relaxation :Theory and in Vivo MRS and MRI Applications”, p.55

R49 L.H. Chang and T.LJames, “NMR Methods in Studies of Brain Ischemia”, P.135

R50 S.K. Miller and G.A. Elgavish, “Shift Reagent Aided 23Na NMR Spectroscopy in Cellular, Tissue and Whole-Organ Systems”, p.159

R51 B.S. Selinsky and C.T. Burt, “In Vivo19F NMR”, p.241

R52 R.E. London, “In Vivo2H NMR Studies of Cellular Metabolism”, p.277

R53 L.J. Berliner and H. Fujii, “Some Applications of ESR to In Vivo Animal Studies and EPR Imaging”, p.307

1993, vol.12

R54 G.N. La Mar and J.S. de Ropp,” NMR Methodology for Paramagnetic Proteins”, p.1

R55 L. Banci, “Nuclear Relaxation in Paramagnetic Metalloproteins”, p.79

R56 C.C. Lester and R.G. Bryant, “Paramagnetic Relaxation of Water Protons”, p.113

R57 F.A. Walker and u. Simonis,” Proton NMR Spectroscopy of Model Hemes”, p.133

R58 J.D. Satterlee, S. Alam, Q. Yi, J.E. Erman, I. Constantinidis, D.J. Russell and S.J. Moench,” Proton NMR Studies of Selected Paramagnetic Heme Proteins”, p.275

R59 J. Mispelter, M. Momenteau and J.M. Lhose,” Heteronuclear Magnetic Resonance: Applications to Biological and Related Paramagnetic Molecules”, p.299

R60 C. Luchinat and S. Ciurli,” NMR of Polymetallic Systems in Proteins”, p.357 1993, vol.13

R61 B.J. Gaffney and H.J. Silverstone,” Simulation of the EMR Spectra of High Spin Iron in Proteins”, p.1

R62 P.G. Debrunner,” Moessbauer Spectroscopy of Iron Proteins”, p.59

R63 R. Basosi, W.E. Antholine and J.S. Hyde,” Multifrequency ESR of Copper: Biophysical Applications”, p.103

R64 B.M. Hoffman, V.J. DeRose, P.E. Doan, R.J. Gurbiel, A.L.P. Houseman and J. Telser,” Metalloenzyme Active Site Structure and Function through Multifrequency CW and Pulsed ENDOR”, p.151

R65 J. Huettermann,” ENDOR of Randomly Oriented Mononuclear Metalloproteins”, p.219

R66 K. Moebius,” High Field EPR and ENDOR on Bioorganic Systems”, p.253

R67 H. Thomann and M. Bernardo,” Pulsed Electron Double and Multiple Resonance Spectroscopy of Metals in Proteins and Enzymes”, p.275

R68 D.C. Thomas, E.M. Ostap, C.L. Berger, S.M. Lewis, P.G. Fajer and J.E. Mahaney,” Transient EPR of Spin-Labeled Proteins”, p.323

R69 A. Tomasi and A. Iannone, “ESR Spin-Trapping Artifacts in Biological Model Systems”, p.353

Bulletin Of Magnetic Resonance, 1993, vol.15

R70 G.C. Leo, R.P. Shank and H.R. Zielke,” The Study of Rat Brain Metabolic Pathways by 13C NMR”, p.8

R71 A.M. Rossi, D.S. Schramm, O. Chaix and G. Poupeau,” Thermal Stability of Trapping Centres in Natural Aragonites”, p.14

R72 J.K. Bonesteel, I. Al-Bala’a and R.D. Bates,” EPR and NMR Studies of Transient Complex Formation of Chloroform with Nitroxide Free Radicals”, p.18

R73 R.K. Harris, D.C. Apperley, N.A. Davies and R.D. Fischer, “High Resolution Solid State NMR of Organometallic Coordination Polymers”, p.22

R74 S.G. Kim, M. Salazar and B.R. Ried,” Automatic NOE Back Calculation”, p.29

R75 T. Takui, Y. Teki, M. Endoh, H. Kitai, Y. Okudo, S. Kita, T. Kinoshita and K. Itoh, “Organic High Spin State ENDOR/TRIPLE Spectroscopy”, p.41

R76 A.M. Rossi, N.M. Pinhal and N.V. Vugman,”Evidence of Rotating CO2- Radicals in Bioapatites of Calcified Tissue”, p.48

R77 D.M. Wang, I. Kovacik, E.J. Reijerse and E. deBoer,” Structural Change in (NH4)2[Zn(NH3)2(CrO4)2] and (NH4)2[CdNH3)2(CrO4)2] Doped with Cu(II), Observed with EPR”, p.50

R78 R.J. Buist, M. Novak, C. Hudspeth and B.J. Blackburn, “Vivo31P NMR Spectra of the Liver Region of Mice Infected with Hymenolepis Microstoma and Mesocestoides Vogae”, p.55

R79 D.S. Williams J.A. Detre, W. Zhang and A.P. Koretsky,” Fast Serial MRI of Perfusion in the Rat Brain Using Spin Inversion of Arterial Water”, p.60

R80 A.D. Bain and G.J. Duns, “Equivalence of Pulsed and Continuous Radiation in NMR”, p.64

R81 N.J. Clayden, “Morphology in Peek by NMR Relaxation Time Measurements”, p.70

R82 C.M. Preston, B.G. Sayer and R.H. Newman, “NMR and Forest Ecosystem Dynamics”, p.75

R83 N. Zhou and H.J. Vogel,” d(T8C4A8) Forms a Hairpin with a Bent Stem and an Unstacked Cytosine”, p.80

R84 J.M. Aramini and H.J. Vogel,” Quadrupolar Metal Ion NMR to Probe Metal Binding to Proteins: 27A NMR Studies of Ovotransferrin”, p.84

R85 L.A. Denys, A.J. Williams and G. Sachs,” 2D Hetero and Homonuclear NMR Study of a K+ Competitive Fluorescent Inhibitor of the H,K-ATPase”, p.89

R86 Y. Kuroda, M. Wakita and T. Nakagawa, “Interaction Between Dibucaine and Pig Erythrocyte Membranes as Studied by NOESY Experiments in 1H NMR Spectroscopy”, p.93

R87 M. Zhang and H.J. Vogel, “Protein Engineering and NMR Studies of Lysine Residues in Mammalian Calmodulin”, p.95

R88 H. Fukui, M. Miura and H. Matsuda, “Gauge Invariant Many Body Perturbation Calculations of Nuclear Magnetic Shieldings”, p.98

R89 K. Furukawa, T. Matsumura, Y. Teki, T. Kinoshita, T. Takui and K. Itoh,” Molecular Design, Synthesis and ESR Detection of a Ground State Tridecet Hydrocarbon as a Model for 2D Organic Ferro- and Superpara-Magnets”, p.103

R90 Y. Inagaki, H. Maekawa, T. Yokokawa and S. Shimokawa,” High Temperature NMR Studies of Sodium Borates”, p.108

R91 A. Diaz, R. Monque and M. Bussolo,” Quantitative Determination of Gallium in Zeolites by 71Ga MAS NMR Spectroscopy”, p.112

R92 M.R. Morrow, D. Lu, D. Singh and C.W.M. Grant,” NMR Studies of Phase Behaviour and Chain Orientational Order in Glycosphingolipid-Phosphatidylcholine Mixtures”, p.117

R93 T. Pott and E.J. Dufourc,” Cholesterol Inhibits Melittin-Induced Membrane Lysis”, p.121

R94 A, Leonard, A. Milon, M.A. Krajewski-Bertrand and E.J. Dufourc,” Modulation of Membrane Hydrophobic Thickness by Cholesterol, Cycloartenol and Hopanoid”, p.124

R95 R.S. Phadke, S. Arivastava and G. Govil,” Antioxidants in Biomembranes: Magnetic Resonance Studies”, p.128

R96 V.A. Silaev, K.M. Mysin, O.I. Gnezdilov, E.S. Nefed’ev, L.A. Abrakhinanova and V.G. Khozin,” New Results in the Investigations of Polymers by EPR and EPR-Tomography”, p.133

R97 L.J. Berliner and J.K. Woodford,” Interactions of Hirudin Analogues with Bovine and Human THrombins”, p.142

R98 T. Nakai and C.A. McDowell,”The NMR Spectra of Homonuclear Two-Spin Systems Under Magic Angle and Off-Magic Angle Spinning”, p. 149

R99 M.R. Merrill,” Coreflood Experiments on Casper Sandstone”, p.154

R100 D.G. Cory and W.E. Maas, “NMR Imaging of Solid Polymers”, p.160

R101 R. Ricciolini, A. Miccheli, E. Piccolella, A. Tomassini, C. Manetti, M.E. DiCocco and F. Conti, “Biochemical and Biophysical Effects of Dexamethasone on Human Lymphoblastoid Cell Lines, Studies by 31P and NMR Spectroscopy and Fluorimetry”, p.165

R102 T. Aureli, G. Capuani, M.E. Di Cocco, A. Miccheli, N. Corsico, A. Nardone, E.A. Martelli and F. Conti,” Peripheral Arteriopathy in the Rat”, p.169

R103 P.M. Debenham, P.J. McDonald, A.J. Horsewill and D. Vijayaraghavan,” Tunnel Splitting of 2,3 Butanedione with Pressure Studied using Low Field NMR Tunnelling Spectroscopy”, p.172

R104 L.C. terBeek and E.E. Bumell, “Spin-Lattice Relaxation for Dideuterium”, p.175

R105 C.A. Fyfe, J. Niu, S. Rettig, N.E. Burlinson, CReidsma, D. Wang and M. Poliks, “High Resolution and ^N NMR Investigations of the Curing Reaction of Cyanate Resins”, p.179

R106 E. Brosio, E. Camovale, M. Delfini, L. Pizzoferrato and G. Veglia,” 31P NMR Study on Phytase Catalysed Hydrolysis of Phytate”, p.183

R107 L.J. Mueller and D.P. Weitekamp,” Molecular Beam Magnetic Resonance via the Longitudinal Stem Gerlach Effect”, p.187

R108 S.K. Buratto, J.Y. Hwang, N.D. Kurur, D.N. Shykind and D.P. Weitekamp,” FT Time Sequenced Optical NMR of Gallium Arsenide”, p.190

R109 C.A. Fyfe, P.P. Aroca and Y. Zhang,” NMR Characterization of the Homopolymers and Copolymers Formed from Tetraethoxysilane and Methyltriethoxysilane in a Sol-Gel Process”, p.195

R110 T. Chandrakumar and E.E. Burnell,” Comparison of Short Range Interactions in Zero Electric Field Gradient Mixtures”, p.199

Rill S.R. Wassall, S. Ayalasomayajula, G.L. Grffith, M.A. McCabe, W.D. Ehringer and W. Stillwell,” 2H NMR Studies of Membrane Stabilization by Vitamin E”, p.205

R112 S.J. Hwang and B.C. Gerstein,” Spin Counting in Dipolar Coupled Spin 1/2 Systems by Multiple Quantum Coherence”, p.211

Chemical Reviews, 1993, vol.93

(Continues…)Excerpted from Nuclear Magnetic Resonance Volume 24 by G. A. Webb. Copyright © 1995 The Royal Society of Chemistry. Excerpted by permission of The Royal Society of Chemistry.
All rights reserved. No part of this excerpt may be reproduced or reprinted without permission in writing from the publisher.
Excerpts are provided by Dial-A-Book Inc. solely for the personal use of visitors to this web site.