Nuclear Magnetic Resonance Volume 23

A Review of the Literature Published Between June 1992 and May 1993

By G. A. Webb

The Royal Society of Chemistry

Copyright © 1994 The Royal Society of Chemistry
All rights reserved.
ISBN: 978-0-85186-462-4

Contents

CHAPTER 1 NMR Books and Reviews By G.A. Webb, 1,
CHAPTER 2 Theoretical and Physical Aspects of Nuclear Shielding By C.J. Jameson, 47,
CHAPTER 3 Applications of Nuclear Shielding By M. Yamaguchi, 79,
CHAPTER 4 Theoretical Aspects of Spin-Spin Couplings By H. Fukui, 124,
CHAPTER 5 Applications of Spin-Spin Couplings By K. Kamienska-Trela, 137,
CHAPTER 6 Nuclear Spin Relaxation in Liquids By H. Weingärtner, 179,
CHAPTER 7 Solid State NMR By K.D.M. Harris and A.E. Aliev, 206,
CHAPTER 8 Multiple Pulse NMR By L. Y. Lian, 245,
CHAPTER 9 Natural Macromolecules By J.R.P. Arnold and J. Fisher, 272,
CHAPTER 10 Synthetic Macromolecules By A.H. Fawcett, 306,
CHAPTER 11 Conformational Analysis By J. Barber and B. Wood, 328,
CHAPTER 12 Nuclear Magnetic Resonance Spectroscopy of Living Systems By M.J.W. Prior, 366,
CHAPTER 13 Nuclear Magnetic Resonance Imaging By S. C.R. Williams, 407,
CHAPTER 14 Oriented Molecules By C.L. Khetrapal and K, V. Ramanathan, 439,
Author Index, 465,

CHAPTER 1

NMR Books and Reviews

COMPILED BY G. A. WEBB

The section lists all books and reviews, with n.m.r. as the principal theme, that were known to the compiler, for the period under review. In most cases the source of references is the ‘CA Selects-NMR Chemical Aspects’ listings for the period from June 1992 to May 1993. References to technical bulletins, company or institute house journals, special reports, etc., are normally omitted. In general, texts of individual lectures from symposia are not listed nor are n.m.r. sections of general chemistry or spectroscopy textbooks. The compilation is sectionalized for the reader’s convenience. The foreign language articles are grouped together according to language and the English title is provided.

(a) BOOKS

R1 A.V.U. Atta-ur-Rahman, “13CNMR of Natural Products”, Volume 1 Monoterpenes and Sesquiterpenes, Plenum Press, New York, 1991, 967pp

R2 A.V.U. Atta-ur-Rahman, “13C NMR of Natural Products”, Volume 2, Diterpenes, Plenum Press, New York, 1991, 795pp

R3 J.K.M. Sanders and B.K. Hunter, “Modern NMR Spectroscopy”, Hirokawa Publishing Co., Tokyo, 1992,403pp

(b) REGULAR REVIEW SERIES

Accounts of Chemical Research, 1992, Vol. 25

R4 E.W. Wooten, K.T. Muller and A. Pines, “New Angles in NMR Sample Spinning”, p.209

Advances in Carbohydrate Analysis, 1991, Vol. 1

R5 C. Jones, “NMR Methods for the Structural Analysis of Polysaccharides and Glycoprotein Carbohydrate Chains”, p.145

Advances in Chemistry Series, 1992, Vol. 230

R6 R. Whyman, “In situ Spectroscopic Studies in Homogeneous Catalysis”, p.19

Advances in Colloid and Interfacial Science, 1992, Vol.42

R7 T. Cosgrove and P.C. Griffiths, “NMR Studies of Adsorbed Polymer Layers”, p.175

Advances in Experimental and Medical Biology, 1991, Vol.302

R8 S.J. Schmidt and H.M. Lai, “Use of NMR and MRI to Study Water Relations in Foods”, p.405

R9 S.J. Schmidt, “Determination of Moisture Content by Pulsed NMR Spectroscopy”, P.599

Advances in Magnetic and Optical Resonance, ed. W.S. Warren, 1992, Vol.17

R10 J. Paff, B. Bluemich and R. Kaiser, “Nonlinear Incoherent Spectroscopy: NOISY”, p.1

R11 Y.A. Serebrennikov, “Zero Field Spin Dynamics and Relaxation”, p.47

Annual Reports on NMR Spectroscopy, ed. G.A. Webb, 1993, Vol.25

R12 M. Witanowski, L. Stefaniak and G.A. Webb, “Nitrogen NMR”, p.1 1993, Vol.26

R13 P.S. Belton, I.J. Colquhoun and B.P. Hills, “Applications of NMR to Food Science”, p.1

R14 A. Shoji, S. Ando, S. Kuroki, I. Ando and G.A. Webb, “Structural Studies of Peptides and Polypeptides in the Solid State by 15N NMR”, p.55

R15 K. Hatada, “Application of High Resolution NMR Spectroscopy to Polymer Chemistry”, p.99

R16 J.L. Allis, “The Application of Cation NMR to Living Systems : 87Rb NMR”, p.211

R17 A. Lycka, “Multinuclear NMR of Azo Dyestuffs”, p.247

Annual Reviews of Biophysics and Biomolecular Structure, 1992, vol.21

R18 S.O. Smith and O.B. Peersen, “Solid State NMR Approaches for Studying Membrane Protein Structure”, p.25

R19 G. Wagner, S.G. Hyberts and T.F. Havel, “NMR Structure Determination in Solution”, p.167

R20 W.S. Englander and L. Mayne, “Protein Folding Studied using Hydrogen Exchange Labeling and 2D NMR”, p.243

Annual Reviews of Physiology, 1992, vol.54

R21 R.J. Gillies, “NMR and its Applications to Physiological Problems”, p.733

R22 N.E. Mackenzie, P.R. Gooley and L.A. Hardaway, “Solving Solution Structures of Physiologically relevant Proteins by NMR Spectroscopy”, p.749

R23 B.S. Szwergold, “NMR Spectroscopy of Cells”, p.775

R24 A.P. Koretsky and D.S. Williams, “Applications of Localized in vivo NMR to Whole Organ Physiology in the Animal”, p.799

Biological Magnetic Resonance, ed. L.J. Berliner and J. Reuben, 1992, vol.10

R25 J.P. Kamerling and J.F.G. Vliegenthart, “High Resolution 1H NMR

Spectroscopy of Oligosaccharide-alditall released from Mucin type o-Glycoproteins”, p.1

R26 D.E.Wemmer, “NMR Studies of Nucleic Acids and their Complexes”, p.195

Bulletin Of Magnetic Resonance, 1992, vol. 13

R27 V.J. Kowalewski, “On the Effect of a Negative Resistance Circuit on a NMR Sample”, p.72

R28 S.S. Eaton and G.R. Eaton,” Quality Assurance in EPR”, p.83

R29 J.F. Hinton, “Thallium NMR Spectroscopy”, p.90

R30 P.A. Mirau, “2D NMR Studies of Synthetic Polymers”, p.109 1992, vol.14

R31 K.T. Mueller, C.A. Fyfe, H. Grondey, K.C. Wong-Moon and T. Markus, “Solid State Polarization Transfer Experiments Involving Quadrupolar Nuclei”, p.9

R32 I.P. Goudemond, G.J. Hill and M.J.R. Hoch, “Magnetic Resonance Evidence for Superconductivity in a Semimetal”, p.12

R33 R. Deslauriers, S. Lareau, R.S. Labow, W.J. Keon, G.H. Tian, A.L. Panos, C.A.M. Barrozo, I.S. Ali, O.Al-Nowaiser and T.A. Salerno, “NMR Spectroscopy in Cardiac Surgery”, p.15

R34 Y. Teki, K. Sato, M. Okamoto, A. Yamashita, Y. Yamaguchi, T. Takui, T. Kinoshita and K.ltoh, “Topology and Spin Alignment in Organic High Spin Molecules”, p.24

R35 C. Mailer, B.H. Robinson and D.A. Haas, “New Developments in Pulsed EPR: Relaxation Mechanisms of Nitroxide Spin Labels”, p.30

R36 D.A. Haas, C. Mailer, T. Sagano and B.H. Robinson, “New Developments in Pulsed EPR : Direct Measurement of Rotational Correlation Times from Decay Curves”, p.35

R37 R.C.R. Grace and A. Kumar, “Non-Linear Effects in Standard 2D NOE Experiments in Coupled Spin Systems”, p.42

R38 D.A. Keire and D.G. Gorenstein, “Deriving Structures from 2D NMR”, p.57

R39 H.Senn, W.Klaus and P.Gerber, “3D Structure Determination of Flavoridin in Solution”, p.64

R40 L.Y. Lian, J.P. Derrick, V.Ramesh, R.O. Frederick, S.E.H. Syed and G.C.K. Roberts, “NMR Approaches to Large Proteins”, p.65

R41 S. Mohanty, L.C. Sieker and G.P. Drobny, “2D NMR Study of Drug-Protein Interactions”, p.68

R42 F. Ni, “Quantitative Analysis in Multi Dimensional Transferred NOE Experiments” ,p.75

R43 J.N.S. Evans, R.J. Appleyard and W. Shuttleworth, “Time Resolved Solid State NMR: Small Molecules and Enzymes in Rapidly Frozen Solution”, p.81

R44 M.R. Johnson, S. Clough, A.J. Horsewill and I.B.I. Tomsah, “Coupled Methyl Groups in Dimethyl Sulphide”, p.86

R45 P.A. Shaw, W.R. Carper, C.E. Keller and J.S. Wilkes, “NMR Relaxation Studies of Microdynamics in Chloroaluminate Melts”, p.92

R46 T.A. Cross, R.R. Ketchem, W. Hu, K.C. Lee, N.D. Lazo and C.L. North, “Structure and Dynamics of a Membrane Bound Polypeptide”, p.96

R47 E. Gaggelli, N. Gaggelli, G. Valensin and A. Maccotta, “The Role of Metal Ions in Processes of Conformational Selection during Ligand-Macromolecule Interactions”, p.102

R48 L.H. Randall, C.A. Fyfe, Z. Mei and S. Whitworth, “Detection and Characterization of CFC, HCFC and HFC Gases in Foamed Insulation by High Field NMR Imaging”, p.108

R49 C.Szantay, “Mysterious Negative Peaks in the 1H{1H}NOE Difference Spectra of some Thiopyran Compounds”, p.112

R50 A. Yoshino, K. Aoki, M. Ushio and K. Takahashi, “1H and 13C NMR Spectra of the Carbanions Produced from Phenylpropene Derivatives”, p.116

R51 E.R. Barton-Davis, R.W. Wiseman and M.J. Kushmerick, “Intracellular pH and Inorganic Phosphate Effects on Skeletal Muscle Force”, p.122

R52 M. Goldman, T. Tabti, C. Fermon, J.F. Jacquinot and G. Saux, “A Simple Model for the Influence of Motion on the NMR Line shape”, p.126

R54 J. Sun and A. Watton, “The Effect on T1 of Correlated Water Motions in the Polar Phase of Colemanite”, p. 131

R55 R.Y. Dong, “Measurement of Deuteron Spin Relaxation Times in Liquid Crystals by a Broadband Excitation Sequence”, p.134

R56 A.A. Rodriguez, T. Davis and L.E. Nance,” 13C Relaxation Mechanisms and Motional Studies in Selected Halomethane Molecules”, p.139

R57 R.J. Pugmire, Y.J. Jiang, M.S. Solum and D.M. Grant, “An Efficient Large Sample Volume System for Solid State NMR”, p.144

R58 D.W. Lowman and D.R. Fagerburg, “Magnetic Resonance Spectroscopic Investigations of poly(p-Phenylene Sulphide/Disulphide)”, p.148

R59 S. Kaplan, “Application of 2D HETCOR NMR to Investigate Polymer Blend Heterogeneity”, p.153

R60 M.T. Nunes, A. Vainrub, M. Ribet, F. Rachdi, P. Bemier, M. Almeida and G. Feio, “New High Resolution NMR Studies in Polycrystalline Teracyanoquinodimethane”, p.156

R61 C.S. Modi, E. McLaughlin, D.S. Bendall, S. He and J.C. Gray, “Use of NMR Relaxation Measurements to Derive the Binding Site of Plastocyanin in Complexes with Cytochrome-F”, p.159

R62 A. Spisni, G. Sartor, L. Franzoni, A. Orsolini, P. Cavatorta and M. Tabak, “Metal-peptide Interactions”, p.165

R63 J.N.S. Evans, M.S. Nissen and R. Reeves, “Assignments of the 1H NMR Spectrum of a Consensus DNA-Binding Peptide from the HMG-I Protein”, p.171

R64 J.D. Baleja, V. Thanabal, T. Mau and G. Wagner, “Solution Structure of the DNA Binding Domain of GAL4 from Saccharomyces cerevisiae“, p.175

R65 C. Rossi, A. Donati, S. Ulgiati and M.R. Sansoni, “Structural Investigation of Folic Acid by NMR Relaxation and Molecular Mechanics Analysis”, p.181

R66 L.H. Randall, G.E. Sedgewick and C.A. Fyfe, “Characterization of Water in Bitumen Emulsions in Model Porous Media by NMR Microscopic Imaging Techniques”, p.186

R67 J. Callahan, D. Mattiello and G.P. Drobny, “Computer Graphics for Pulse Sequence Analysis”, p.191

R68 C. Rossi, A. Lepri, M.P. Picchi, S. Bastianoni, D. Medaglini, M. Vanassina and E. Cresta, “NMR Investigation of the Simultaneous Fermentation of Xylose and Glucose by a Selected Strain of Klebsiella planticola (G11)”, p.197

R69 B.J. Stockman, T.A. Scahill, A. Euvrard, N.A. Strakalaitis, D.P. Brunner, A.W. Yem and M.R. Deibel, “Interleukin-1 Receptor Antagonist Protein”, p.202

R70 M.Martin-Landrove and J.A. Moreno, “Green’s Function Calculation of Effective Nuclear relaxation Times in Metals and Disordered Metals”, p.208

R71 D.H. Jones, N.D. Kurur and D.P. Weitekamp, “Stochastic Averaging Revisited”, p.214

R72 P.J. Pizarro and D.P. Weitekamp, “Magnetic Resonance of Trapped Ions by Spin Dependent Cyclotron Acceleration”, p.220

R73 R. Basosi, R. Pogni and C.D. Lunga, “Coordination Modes of Histidine Moiety in Copper (II) Dipeptide Complexes Detected by Multifrequency EPR”, P.224

R74 M. Geoffroy, G. Terron, A. Jouaiti, P. Tordo and Y. Ellinger, “An EPR and ab initio Study of a Fhosphaalkene Radical Anion and Comparison with other Phosphorus Containing Radical Ions”, p.229

R75 A.R. Bizzam and S. Cannistraro, “Conformational Substrate Distribution in Myoglobin as Studied by EPR Spectroscopy”, p.234

R76 A.R. Lim, C.S. Kim and S.H. Choh, Effect of Paramagnetic Ions in Aqueous Solution for Precision Measurement of the Proton Gyromagnetic Ratio”, p.240

R77 S.H. Choh and K.T. Han, “Magnetic Resonance of 23Na and 14N Nuclei in Single and Multi Domain Crystals of Ferroelectric NaNO2”, p.246

R78 M.J.R. Hoch and S.T. Stoddart, “Knight Shifts and Spin Dynamics in Disordered Systems”, p.252

R79 D.L. Mattielo, J. Callahan, T. Alam and G.P. Drobny, “Numerical Design and Evaluation of Broadband Pulse Sequences for I = 1 Spin Systems”, p.255

R80 S. Mammi, “A BASIC Program to Calculate the Evolution of Cartesian Product Operators”, p.259

R81 T. Parella, F. Sanchez-Ferrando and A. Virgili, “Selective Long Range Polarization Transfer via DEPT”, p.263

R82 S.A. Smith, W.E. Palke and J.T. Gerig, “Computer Simulations of High Resolution NMR Spectra”, p.267

R83 I.J. Shannon, K.D.M. Harris and S. Arumugam, “Variation of 13C NMR Linewidths of Metallocenes as a Function of MASS Frequency”, p.273

R84 J. Kuemmerlen, T. Schaller, A. Sebald and H. Keppler, “The Structural Role of Water in Silicate Glasses”, p.278

R85 S. Hayashi, T. Ueda, K. Hayamizu and E. Akiba, “High Resolution Solid State NMR Study of Microstructures in Layered Aluminosilicate”, p.282

R86 C. Connor, “Broadline NMR of Structural Ceramics”, p.285

R87 F.G. Herring, W.R. Cullen, J.C. Nelson and P.S. Phillips, “Permeability of Liposomal Membranes to Molecules of Environmental Interest”, p.289

R88 L.Ma, T.F. Taraschi and N. Janes, “NMR Partitioning Studies of Solute Action in Lipid Membranes”, p.293

R89 C.L. Khetrapal, “Weak Molecular Interactions: NMR Spectroscopy of Oriented Molecules”, p.299

R90 R.J. Wittebort and A.M. Clark, “Structural Studies of Collagen by Solid State NMR”, p.303

Chemical Reviews, 1992, vol.92

R91 S. Li and W.C. Purdy, “Cyclodextrins and their Applications in Analytical Chemistry”, p.1457

Chemical Society Reviews, 1992, vol.21

R92 M. Williamson and J.P. Waltho, “Peptide Structure from NMR”, p.227

Coordination Chemistry Reviews, 1992, vol.114

R93 J.A. Davies, “Solid State 31P NMR Spectroscopic Studies of Tertiary Phosphines and their Complexes”, p.61

R94 J.A. Davies and S. Dutremeg, “Solid State NMR Studies of d-block and p-block metal nuclei”, p.201

1992, vol.l20

R95 L. Banci, M. Piccioli and A. Scozzafava, “Advances in the NMR Investigations of Paramagnetic Molecules in Solution”, p.1

R96 C. Luchinat and Z. Xia, “Paramagnetic and Dynamic Properties of Electrons and Nuclei”, p.281

Magnetic Resonance Reviews, ed. C.P. Poole, 1991, vol.16

R97 V.A. Atsarkin, “Spin Dynamics of Paramagnetic Impurities in Solids”, p. 1

R98 C.L. Khetrapal and E.D. Becker, “NMR of Oriented Molecules”, p.35

R99 S.K. Misra and J.S. Sun, “EPR Studies of Mn2+ in Single Crystals and Powders”, p.57

R100 H. Figiel, “NMR of Magnetic Materials”, p.101

NMR Basic Principles and Progress, ed. P. Diehl, S. Fluck, H. Guenther, R. Kosfeld and J. Seelig, 1992, vol.26

R101 J. Link, “The Design of Resonator Probes with Homogeneous Radiofrequency Fields”, p.1

R102 M. Schnall, “Probes Tuned to Multiple Frequencies for In vivo NMR”, p.33

R103 P.C.M. van Zijl and C.T.W. Moonen, “Solvent Suppression Strategies for In vivo Magnetic Resonance Spectroscopy”, p.67

R104 M. Garwood and K. Ugurbil, “B1 Insensitive Adiabatic RF Pulses”, p.109

R105 P.G. Morris, “Frequency Selective Excitation using Phase Compensated RF Pulses in One and Two Dimensions”, p.149

R106 S. Mueller, “RF Pulses for Multiple Frequency Excitation: Theory and Application”, p. 171

R107 R. de Beer and D. van Ormondt, “Analysis of NMR Data Using Time Domain Fitting Procedures”, p.201

R108 E.B. Cady, “Determination of Absolute Concentrations of Metabolites from NMR Spectra”, p.259

1992, vol.27

R109 C.S. Bosch and J.J.H. Ackerman, “Surface Coil Spectroscopy”, p.3

R110 P. Styles, “Rotating Frame Spectroscopy and Spectroscopic Imaging”, p.45

R111 P.A. Bottomley, “Depth Resolved Surface Coil Spectroscopy DRESS”, p.67

R112 R.J. Ordidge and J.A. Helpem, “Image Guided Volume Selective Spectroscopy: A Comparison of Techniques for In vivo31P NMR Spectroscopy of Human Brain”, p.103

R113 M. Decorps and D. Bourgeois, “Localized Spectroscopy Using Static Magnetic Field Gradients: Comparison of Techniques”, p.119

R114 J.A. den Hollander, P.R. Luyten and A.J.H. Marien, “1H NMR Spectroscopy and Spectroscopic Imaging of the Human Brain”, p. 151

R115 H.P. Hetherington, “Homo and Heteronuclear Editing in Proton Spectroscopy”, p.179

(Continues…)Excerpted from Nuclear Magnetic Resonance Volume 23 by G. A. Webb. Copyright © 1994 The Royal Society of Chemistry. Excerpted by permission of The Royal Society of Chemistry.
All rights reserved. No part of this excerpt may be reproduced or reprinted without permission in writing from the publisher.
Excerpts are provided by Dial-A-Book Inc. solely for the personal use of visitors to this web site.