Nuclear Magnetic Resonance Volume 22

A Review of the Literature Published Between June 1991 and May 1992

By G. A. Webb

The Royal Society of Chemistry

Copyright © 1993 The Royal Society of Chemistry
All rights reserved.
ISBN: 978-0-85186-452-5

Contents

CHAPTER 1 NMR Books and Reviews By G.A. Webb, 1,
CHAPTER 2 Theoretical and Physical Aspects of Nuclear Shielding By C.J. Jameson, 59,
CHAPTER 3 Applications of Nuclear Shielding By I.P. Gerothanassis, C. Efthimiou, and C. Vakka, 90,
CHAPTER 4 Theoretical Aspects of Spin-Spin Couplings By H. Fukui, 138,
CHAPTER 5 Applications of Spin-Spin Couplings By K. Kamienska-Trela, 159,
CHAPTER 6 Nuclear Spin Relaxation in Liquids By H. Weingartner, 197,
CHAPTER 7 Solid State NMR By K.D.M. Harris, 230,
CHAPTER 8 Multiple Pulse NMR By L.Y. Lian, 261,
CHAPTER 9 Natural Macromolecules By H.G. Parkes, 290,
CHAPTER 10 Synthetic Macromolecules By A.H. Fawcett, 333,
CHAPTER 11 Conformational Analysis By C. Jones, 346,
CHAPTER 12 Nuclear Magnetic Resonance Spectroscopy of Living Systems By P.G. Morris, 374,
CHAPTER 13 Nuclear Magnetic Resonance Imaging By S.C.R. Williams, 416,
CHAPTER 14 NMR of Paramagnetic Species By P.-O. Westlund, 454,
CHAPTER 15 NMR of Liquid Crystals and Micellar Solutions By A. Khan, 498,
Author Index, 541,

CHAPTER 1

NMR Books and Reviews

COMPILED BY G. A. WEBB

The section lists all books and reviews, with n.m.r. as the principal theme, that were known to the compiler, for the period under review. In most cases the source of references is the ‘CA Selects – NMR Chemical Aspects’ listings for the period from June 1991 to May 1992. References to technical bulletins, company or institute house journals, special reports, etc., are normally omitted. In general, texts of individual lectures from symposia are not listed nor are n.m.r. sections of general chemistry or spectroscopy textbooks. The compilation is sectionalized for the reader’s convenience. The foreign language articles are grouped together according to language and the English title is provided.

(a) BOOKS

R1 M. Goldman, “Quantum Description of High Resolution NMR in Liquids”, Oxford University Press, 1990, 288pp.

R2 R. Kitamaru, “NMR: Principles and Theory”, Elsevier, Amsterdam, 1990, 211pp.

R3 M. Munakata, S. Kitagawa and S. Shibata, “Introduction to Polynuclear NMR”, Kodansha Ltd., Tokyo, 1991, 334pp.

(b) REGULAR REVIEW SERIES

Aacounts of Chemical Research, 1991, Vol. 24.

R4 J.D. Puglisi, J.R. Hyatt and I. Tinoco, “ENA Pseudoknots”, P.152.

1991, Vol. 25.

R5 F. Diederich and R.L. Whetten, “Beyond C60: the higher fullerenes”, P.119.

Advances in Biophysical Chemistry, 1990, Vol. 1.

R6 B.J. Stockman and J.L. Markley, “Stable Isotope Assisted Protein NMR in Solution”, P.1.

R7 D.G. Gorenstein, R.P. Meadows, J.T. Metz, E. Nikonowicz and C.B. Post, “31p and 2D NMR and NOESY distance restrained molecular dynamics methodologies”, P.47.

R8 S. Ihuta and Y.S. Wang, “NMR Studies of 3- and 7-DNA Hairpins of d[(CG)3T4(CG)5] in Solution”, P.125.

Advances in Experimental and Medicinal Biology, 1990, vol. 279.

R9 O.P. Kuipers, C.J. Van den Bergh, H.M. Verheij and G.H. De Haas, “Probing the Mechanism of Pancreatic Phospholipase A2 with the aid of recombinant DNA Techniques”, P.65.

Advances in Magnetic and Optical Resonance, ed. w.s. Warren, 1990, Vol.15

R10 R. Tycho, “Iterative Methods in the Design of Pulse Sequences for NMR Excitation”, P.1.

R11 R.A. Wind and H. Loch, “Electron-Nuclear Polarization Transfer in the Nuclear Rotating Frame”, P.51.

R12 B.C. Sanctuary and T.K. Halstead, “Multipole NMR”, P.80.

R13 K.W. Zilm and J.M. Millar, “Solid State and Solution NMR of Nonclassical Transition Metal Polyhydrides”, P.163.

R14 C. Connor, “Low-Frequency Magnetic Resonance with a dc SQUID”, P.201.

1991, Vol. 16.

R15 D. Suter and J. Mlyneh, “Laser Excitation and Detection of Magnetic Resonance”, P.2.

R16 R.R. Void and R.L. Void, “Deuterium Relaxation in Molecular Solids”, P.85.

R17 S. Lacelie, “On the Growth of Multiple Spin Coherences in NMR of Solids”, P.173.

Advances in Molecular Modelling, 1990, vol. 2.

R18 G.R. Painter, J.P. Shochcar and W.C. Andrews, “Applications of Molecular Mechanics to the Study of Drug Membrane Interactions”, P.135.

Advances in Oxygenated Processes, 1991, vol. 3.

R19 A.L. Baumstarh and D.W. Boyhin, “17O NMR Spectroscopy: Applications to

Structural Problems in Organic Chemistry”, P.141.

Annual Reports on NMR Spectroscopy, ed. g.a. Webb, 1992, vol. 24.

R20 N.J. Claydon, “Developments in Solid State NMR”, P.2.

R21 D.G. Corey, “Solid State NMR Imaging”, P.88.

R22 J. Grandjean, “NMR Studies of Interfacial Phenomena”, P.181.

R23 J.C. Veniero and R.K. Gupta, “NMR Measurements of Intracellular Ions in Living Systems”, P.219.

R24 B. Wrachmeyer and R. Contreras, “199Hg NMR Parameters”, P.267.

R25 W. Meiler and R. Meusinger, “Applications of NMR Methods in Coal Research”, P.331.

Annual Reports on Progress in Chemistry, 1990, vol. 86B.

R26 J.R. Everett and S.A. Readshaw, “High Resolution NMR of Biological Fluids and Biological Macromolecules”, P.3.

1991, Vol. 87C

R27 G.A. Webb, “NMR Spectroscopy”, P.3.

Annual Reviews of Biophysics and Biophysical Chemistry, 1991, vol. 70.

R28 M.G. Clore and A.M. Gronenborn, “2, 3 and 4-dimensional NMR Methods for obtaining Larger and more precise 3-dimensional Structures of Proteins in Solution”, P.79.

Annual Reviews on Materials Science, 1991, vol. 21.

R29 H.W. Spiers, “NMR Methods for Solid Polymers”, P.131.

R30 R.A. Assink and B.D. Kay, “Study of Sol-Gel Chemical Reaction Kinetics by NMR”, P.491.

Annual Reviews of Physical Chemistry, 1991, vol. 42.

R31 C. Dybowski, N. Borsal and T.M. Duncan, “NMR Spectroscopy of Xenon in Confined Spaces”, P.433.

R32 T.L. James and V.J. Basus, “Generation of High Resolution Protein Structures in Solution from Multidimensional NMR”, P.501.

Annual Reviews of Physiology, 1991, vol. 53.

R33 R.E. London, “Methods for the Measurement of Intracellular Magnesium”, P.241.

Bulletin of Magnetic Resonance, 1991, Vol. 13.

R34 D.D. Lasic, “Magnetic Resonance Methods in the Studies of Liposomes”, P.3.

R35 S.J. Nelson, D.M. Schneider, D.L. DeStefano and A.J. Wand, “Refinement and Automation of the Main Chain Directed Assignment Procedure for the Analysis of 2-D 1H Spectra of Proteins”, P.14.

R36 R.P. Meadows, K. Kaluarachchi, C.B. Post and D.G. Gorenstein, “Just How Accurate are Structures Determined from 2D Noesy Spectra? The Morass of an Answer”, P.22.

Chemical Reviews, 1991, vol. 91.

R37 A.R. Derome and S. Bowden, “Low Temperature Solid State NMR of Proteins”, P.1307.

R38 H.W. Spiers, “Structure and Dynamics of Solid Polymers from 2D and 3D NMR”, P.1321.

R39 I.T. Horvath and J.M. Millar, “NMR Under High Gas Pressure”, P.1339.

R40 J.F. Stebbins, “NMR at High Temperatures”, P.1353.

R41 C.J. Jameson, “Gas Phase NMR Spectroscopy”, P.1375.

R42 R. Freeman, “Selective Excitation in High Resolution NMR”, P.1397.

R43 J.J. Led and H. Gesmar, “Application of the Linear Prediction Method to NMR Spectroscopy”, P.1413.

R44 R.K. Harris and P. Jackson, “High Resolution 19F NMR of Solids”, P.1427.

R45 D. Parker, “NMR Determination of Enantiomeric Purity”, P.1441.

R46 J. Klinowski, “Solid State NMR Studies of Molecular Sieve Catalysts”, P.1459.

R47 I. Pelczer and S. Szalma, “Multidimensional NMR and Data Processing”, P.1507.

R48 C.A. Fyfe, Y. Fang, H. Grandey and C.T. Kokotailo, “One and Two Dimensional High Resolution Solid State NMR Studies of Zeolite Lattice Structures”, P.1525.

R49 T.M. Alam and G.P. Drobny, “Solid State NMR Studies of DNA Structure and Dynamics”, P.1545.

Chemical Society Reviews, 1990, vol. 19.

R50 J. Keeler, “2 Dimensional NMR Spectroscopy”, P.381.

Coordination Chemistry Reviews, 1991, vol. 109.

R51 A. Yamasaki, “Solid State NMR of Metal Coordination Complexes and Organometallics”, P.107.

R52 M. Golanka-Cieslak, “Spectroscopy of Cr(VI) Species”, P.223.

1991, Vol. 110.

R53 D. Rehder, “Metal NMR of Organometallic d block Systems”, P.161.

Magnetic Resonance Review, ed. c.p. Poole, 1991, vol. 15.

R54 D. Reinen and M. Atanasov, “The Jahn-Teller Effect and Vibronic Coupling in Transition Metal Chemistry”, P.167.

R55 D.M. Close, “ESR and ENDOR of Irradiated Solids of Biological Interest”, P.24.

NMR Basic Principles and Progress, ed. p. Diehl, E. Fluck, H. Günther, R. Kosfeld and J. Seelig, 1991, Vol. 24.

R56 D. Brinkmann, “Solid State NMR Studies at High Pressure”, P.1.

R57 K.O. Prins, “High Pressure NMR Investigations of Motion and Phase transitions in Molecular Systems”, P.29.

R58 J. Jonas, “High Pressure NMR Studies of the Dynamics in Liquids and Complex Systems”, P.85.

R59 W.Q. Lang and H.-D. Lüdemann, “High Pressure NMR Studies on Hater and Aqueous Solutions”, P.129.

R60 J.W. Akitt and A.E. Merbach, “High Resolution Variable Pressure NMR for Chemical Kinetics”, P.189.

R61 H. Yamada, “Glass Cell Method for High Pressure, High-Resolution NMR Measurements. Applications to the Studies of Pressure Effects on Molecular Conformation and Structure”, P.233.

1991, vol. 25.

R62 R. Freeman and J.B. Robert, “A Brief History of High Resolution NMR”, P.1.

R63 E.W. Bastiaan and C. MacLean, “Molecular Orientation in High-Field High-Resolution NMR”, P.17.

R64 D. Canet and J.B. Robert, “Behaviour of the NMR Relaxation Parameters at High Fields”, P.45.

R65 D. Marion, “Structural Studies of Biomolecules at High Field”, P.91.

R66 U. Haeberlen, “Solid State NMR in High and Very High Magnetic Fields”, P.143.

Progress in NMR Spectroscopy, ed. J.W. Emsley, J. Feeney and L.H. Sutcliffe, 1991, Vol. 23.

R67 P. Jezzard, J.J. Attard, T.A. Carpenter and L.D. Hall, “NMR Imaging in the Solid State”, P.l.

R68 G.M. Clore and A.M. Gronenborn, “Applications of 3- and 4-Dimensional Heteronuclear NMR Spectroscopy to Protein Structure”, P.43.

R69 R. Turner and P. Keller, “Angiography and Perfusion Measurements by NMR”, P.93.

R70 M. Gueron, P. Plateau and M. Decorps, “Solvent Signal Suppression in NMR”, P.135.

R71 r.e. Hoffman and G.C. Levy, “Modern Methods of NMR Data Processing and Data Evaluation”, P.211.

R72 V.M. Mastikhin, I.L. Mudrakovsky and A.V. Nosav, “1H NMR MAS Study of Heterogeneous Catalysis”, P.259.

R73 L.B. Krivdin and E.W. Della, “Spin-Spin Coupling Constants between Carbons separated by more than one bond”, P.301.

1991, Vol. 24.

R74 P.K. Agrawal and D.C. Jain, “13C NMR Spectroscopy of Oleanone Triterpenoids “, P.1.

R75 P.J. Barrie and J. Klinowski, “129Xe NMR as a probe for the Study of Microporous Solids: A Critical Review”, P.91.

R76 A. Majumdar and R.V. Hosur, “Simulation of 2 Dimensional NMR Spectra for the Determination of Solution Conformations of Nucleic Acids”, P.109.

Spectroscopic Properties of Inorganic and Organometallic Compounds, ed. G. Davidson, 1991, Vol. 24.

R77 B.E. Mann, “NMR spectroscopy”, P.l.

(C) EDITED BOOKS AND SYMPOSIA

ACS Symposia Series

R78 D. Hesk, L. Collins, R. Craig and R.O. Mumms, “Athropod Resistant and Susceptible Geraniums”, 1991, 449, 224.

R79 A.J. Douglas and M. Goodman, “Molecular Basis of Taste”, 1991, 450, 128.

R80 W.C. Cheng and K. Rajagopalan, “Selectivity of Silica-Alumina Matrices”, 1991, 452, 198.

R81 R. Sakurovs, L.J. Lynch and W.A. Barton, “Molecular Conformation and Stability of Coal Macerals”, 1991, 461, 111.

R82 P.R. Soloman, M.A. Serio, G.V. Deshpande, E. Kroo, H.H. Schabert and C. Burgess, “Chemistry of Catalytic Preliquifaction”, 1991, 461, 193.

R83 K. Bate and G. Harrison, “Hydrogen Transfer Reactions in Model Systems Representative of Recycle Solvents”, 1991, 461, 236.

AIP Conference Proceedings

R84 J.A. Reynaud, A. Brock, J.P. Grivet and Y. Trudelle, “Interaction of Phospholipids with Basic Amphiphilic Polypeptides”, 1991, 226, 558.

R85 T.L. Aselage and D. Emin, “Structural Model of the Boron Carbide Solid Solution”, 1991, 231, 177.

R86 R.J. Kirkpatrick, T. Aselage, B.L. Phillips and B. Montez, “11b and 13c NMR Spectroscopy of Boron Carbides”, 1991, 231, 261.

R87 G.P. Tsiskarishvili, T. Lundstrom, J. Tegenfelt, T.V. Dolidge and G.V. Tsiskarishvili, “Isotope Effects in $-Rhombohedral Boron”, 1991, 231, 280.

AI Ch E Symposia Series

R88 K.L. McCarthy and J.R. Heil, “Internal Liquid Flow during foam drainage”, 1990, 86, 71.

R89 M.J. McCarthy and J.R. Hell, “Mobility of Hater in Foams Determined by Magnetic Resonance Spectroscopy”, 1990, 86, 102.

Alfred Benzon Symposia

R90 F. Desmoulin, S. Masson, M. Sciaky and P.J. Cozzone, “31p NMR Study of the effects of ethanol Metabolism in the Perfused Rat Liver”, 1991, 30, 464.

R91 S.M. Cohen, “Metabolic Regulation in the Liver as Studied by 13c and 31P NMR of Models of Type 2 Diabetes and Hepatatoxicity”, 1991, 30, 480.

Analysis of Drugs Abuse, ed. T.A. Gough, 1991.

R92 B.A. Dawson, “The Use of NMR Spectroscopy for the Detection and Quantitation of Abused Drugs”, P.283.

Analysis for Drugs and Metabolites, ed. E. Reid and I.D. Wilson, 1990.

R93 F.Y.K. Ghauri, I.D. Wilson and J.K. Nicholson, “19F and 1H NMR Studies of the Metabolism of 4-Trifluoromethyl benzoic acid in the rat”, P.321.

R94 K.E. Wade, I.D. Wilson and J.K. Nicholson, “The Use of 15N NMR in Studying the Metabolism of 15N-labelled Xenobiotics, exemplified by 15N aniline”, P.325.

4th Annual Symposium of the Protein Society, 1990.

R95 R.C. Hoffman and R.E. Klevit, “Structural Analysis of the Amino Terminal Domain of Apo-calmodulin by 1H Homonuclear 2D NMR”, P.383.

Bristol-Myers Squibb/Mead Johnson Nutrition Symposia, 1991, vol. 9.

R96 T.A. Carpenter and L.D. Hall, “Future Prospects for NMR Imaging Spectroscopy in Studies of Human Nutrition”, P.335.

Cellulose, Ed. J.F. Kennedy, G.O. Phillips and P.A. Williams, 1990.

R97 K. Kowsaka, K. Okajima and K. Kamide, “Dependence of Solubility of Cellulose in aqueous alkali solution on the Supermolecular Structure”, P.87.

R98 J. Hayoshi, M. Hoshine and M. Takai, “Two Kinds of 13C NMR Spectra for Cellulose I”, P.119.

R99 F. Horii, A. Hirai and R. Kitamaru, “Structure and Structural Change of Native Cellulose as revealed by CP/MAS 13C NMR Spectroscopy”, P.125.

R100 H. Hatakeyama and T. Hatakeyama, “NMR Relaxation Studies of Water-Cellulose and Water-Sodium Cellulose Sulphate Systems”, P.131.

R101 Y. Tezuka, K. Imai, M. Oshima and T. Chiba, “Determination of Substituent Distribution in Cellulose ethers by means of 13c NMR Studies on their Acetylated derivatives”, P.251.

R102 M.M. Abdel-Malik and M. Yalpani, “Determination of Substituent Distribution in Cellulose ethers by means of 13c NMR Spectroscopy”, P.263.

Chemistry of Amidines and Imidates, ed. S. Patai and z. Rappoport, 1991, Vol. 2.

R103 J. Shorter, “Electronic Effect of Amidino Guanidino and Related Groups”, P.689.

Chemistry of Sulphinic Acids, Esters and their Derivatives, ed. s. Patai and Z. Rappoport, 1991.

R104 A.R. Bassindale and J.N. Iley, “The NMR and ESR Spectra of Sulphinic Acids and their Derivatives”, P.197.

R105 J. Shorter, “Electronic Effects of the Sulphino, SOOH and Related Groups”, P.507.

Chlorophylls, ed. H. Scheer, 1991.

R106 R.J. Abraham and A.E. Rowan, “NMR Spectroscopy of Chlorophyll”, P.797.

1st Conference on Progress in Pacific Polymer Science, 1991.

R107 D.J.T. Hill, D.A. Lewis, J.H. O’Donnell, A.K. Whittaker, D.J. Winzor and C.L. Winzor, “Recent Advances in the Determination of Crosslinking and Scission in Irradiated Polymers”, P.315.

Conformational Forces in Protein Folding, ed. b.t. Noll and K.A. Dill, 1991.

R108 C.M. Dobson, C. Hanley, S.E. Radford, J. Baum and P.A. Evens, “Characterization of Unfolded and Partially folded States of Proteins by NMR Spectroscopy”, P.175.

Developmental Workshop on Carbohydrates from Organic Raw Materials, 1991.

R109 M.A. Clarke, A.V. Bailey, E.J. Roberts and W.S. Tsang, “Polyfructose: a new microbial polysaccharide”, P.169.

4th German, USSR Symposium on Polymer Science, 1990.

R110 V.M. Litvnov, “1H and 2H NMR Study of Chain Motion of Poly(dimethylsiloxane)-filler interface”, P.33.

R111 B.A. Zhubanov, N.Y. Shpil’man, O.A. Almabekov, V.A. Solomin and K.O. Kozybaev, “Navel olicyclic dianhydrides and polyheterocycles and their basis”, P.175.

(Continues…)Excerpted from Nuclear Magnetic Resonance Volume 22 by G. A. Webb. Copyright © 1993 The Royal Society of Chemistry. Excerpted by permission of The Royal Society of Chemistry.
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